Journal Article

·2020

A Novel Imine Based‐Liquid Crystal / PHBHHx Composite: Synthesis and Characterization

Duygu Ceylan‐Erdoğan YTU , Nelisa Türkoğlu Laçin YTU , Hale Ocak YTU , Belkız Bilgin‐Eran YTU

ChemistrySelect

Abstract

Abstract A new imine based chiral calamitic compound carrying a ( S )‐3,7‐Dimethyloctyloxy group at one of terminal was synthesized and characterized by 1 H‐NMR, 13 C‐NMR and FT‐IR spectroscopy. 4‐Dodecyloxybenzylidene‐4′‐(S)‐(3,7‐dimethyloctyloxy) aniline (DBDMA) exhibits an enantiotropic chiral smectic tilted phase (SmC*) at a low temperature range. The mesomorphic properties of new liquid crystal were determined by Differential Scanning Calorimetry (DSC) and Polarised Optical Microscopy (POM). A new composite membrane was also prepared from DBDMA and Poly (3‐hydroxybutyrate‐co‐3‐hydroxyhexanoate) (PHBHHx) via solvent evaporation technique. The surface morphology as well as the mechanical behaviour of PHBHHx/DBDMA composite membrane were investigated by Scanning Electron Microscopy (SEM) and Dynamic Mechanical Analysis (DMA). Additionally, cell compatibility tests of the PHBHHx/DBDMA composite were performed by 3‐(4,5‐Dimethylthiazol‐2‐yl)‐2,5‐diphenyltetrazolium bromide (MTT) method. The surface of PHBHHx/DBDMA composite membrane exhibited a homogenous porosity. The introduction of DBDMA into the polymer media improves the cell viability and mechanical strength.

Keywords

Differential scanning calorimetry Composite number Scanning electron microscope Liquid crystal Materials science Membrane Chemical engineering Polymer chemistry Chemistry Composite material

Subject Areas

Hydrogels: synthesis, properties, applications ·Molecular Medicine ·Life Sciences
Liquid Crystal Research Advancements ·Electronic, Optical and Magnetic Materials ·Physical Sciences

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