Journal Article

·2019

Analysis of Conventionally and Magnetic-Field Dried Fruit and Nuts for Mycotoxins by High-Performance Liquid Chromatography–Tandem Mass Spectrometry (HPLC-MS/MS) and Trace Elements by Inductively Coupled Plasma–Mass Spectrometry (ICP-MS)

Orhan İçelli YTU , Ersoy Öz YTU , Sezgin Bakırdere YTU , Emine Nuroğlu YTU

Analytical Letters

Abstract

A new drying strategy identified as “drying in an oven under a magnetic field” was used for efficient processing of samples. Mycotoxin species and elements (Al, Ba, Co, Cu, Zn, Se, Sr, Mo, Cd, Sn, Pb, Fe, Cr, and Mn) in different foodstuffs (figs, apricots, raisins, hazelnuts, and chilis) were determined using LC-MS/MS and ICP-MS systems at trace levels to evaluate the effectiveness of the new drying method. All of the parameters used in the determination were optimized to obtain efficient determination of analytes. To check the accuracy of the determination methods, proper certified reference materials were used for elemental and mycotoxins contents, and the obtained results were in good agreement with the stated values.

Keywords

Chemistry Chromatography Inductively coupled plasma mass spectrometry Mass spectrometry Mycotoxin High-performance liquid chromatography Certified reference materials Tandem mass spectrometry Analyte Analytical Chemistry (journal) Detection limit Food science

Subject Areas

Heavy Metals in Plants ·Analytical Chemistry ·Physical Sciences
Mycotoxins in Agriculture and Food ·Plant Science ·Life Sciences
Meat and Animal Product Quality ·Animal Science and Zoology ·Life Sciences

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