Journal Article

·2024 OPEN ACCESS

Design, synthesis and anti-oxidant activities of novel 1,2,3,4-tetrazine, 1,2,3-triazoles and coumarin derivatives and their nanoparticular encapsulation

Öznur Eyilcim YTU , Burcu Belmen YTU , Irem Coksu YTU , Serap Acar YTU , Çiğdem Yolaçan YTU , Ömer Tahir Günkara YTU

Nano Express

Abstract

Abstract Nitrogen-containing heterocyclic compounds are currently used for a number of pharmaceutical and agricultural applications because they have biological activities such as antimicrobial, antiviral, antituberculosis, anticancer, analgesic, antioxidant, anti-inflammatory and antidepressant. 1,2,3,4-Tetrazines and 1,2,3-triazoles are examples of high-nitrogen heterocyclic compounds. Coumarins, on the other hand, are lactones that form a group of oxygenated heterocyclic compounds found in plants. In this article, two analogs of 1,2,3,4-tetrazine, two analogs of 1,2,3-triazole and five analogs of coumarin were designed and synthesized. Their chemical structures were characterized by detecting their FTIR, 1 H-NMR, and 13 C-NMR (APT) spectra. The antioxidant activities of all synthesized molecules were compared at a fixed concentration (0.25 mg ml −1 ) using the 1,1-diphenyl-2-picrylhydrazyl (DPPH) method. Molecules 9c and 9e , which showed the highest antioxidant activity, were loaded into PLGA (poly(lactic-co-glycolic) acid) nanoparticles using the oil in water (o/w) single emulsion solvent evaporation method as a model study. Synthesized nanoparticles characterized for particle size, zeta potential, functional groups, morphology, and release properties. Particle size and zeta potential of 9c /NP were determined as 216.1 ± 8.944 nm and −14.1 ± 2.40 mV, respectively. The particle size and zeta potential for 9e /NP were measured as 222.0 ± 12.490 nm and −12.4 ± 1.42 mV respectively. The study results obtained on model nanoparticle systems with elucidated physicochemical properties may have the potential to provide a promising basis for oxidative stress-related diseases in the future.

Keywords

Chemistry Zeta potential Tetrazine DPPH Particle size Antioxidant Nuclear chemistry Carbon-13 NMR Nanoparticle Proton NMR Organic chemistry Nanotechnology Materials science Physical chemistry

Subject Areas

Synthesis and Characterization of Heterocyclic Compounds ·Organic Chemistry ·Physical Sciences
Chemistry and Chemical Engineering ·Environmental Chemistry ·Physical Sciences
Phenothiazines and Benzothiazines Synthesis and Activities ·Molecular Biology ·Life Sciences

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