Journal Article

·2001

Disc-Like Chiral Palladium and Platinum Complexes: Synthesis and Mesomorphic Properties

Belkız Bilgin Eran YTU , D. Singer , Klaüs Praefcke

European Journal of Inorganic Chemistry

Abstract

ortho-Palladated and -platinated benzalimines are a widely studied novel type of liquid-crystals. These sheet-shaped materials contain two or even four metal atoms and carry eight and twelve flexible side-chains, respectively. Here we present the preparation and mesomorphic properties of dinuclear chiral homologues of such sheet-like compounds. On their own, the chiral members of the dinuclear cyclopalladated series exhibit no liquid-crystalline properties, but show mesophase inductions (Colh-phase) in mixtures with an electron-acceptor, e.g., 2,4,7-trinitrofluorenone (TNF). A diplatinated chiral analogue, however, monotropically exhibits the cholesteric nematic discotic (ND*) type of mesophase. Mixtures of this platinum nematogen with TNF also show the induction of a columnar mesophase (Colh) due to charge-transfer interactions.

Keywords

Mesophase Chemistry Palladium Platinum Liquid crystal Crystallography Phase (matter) Acceptor Columnar phase Side chain Discotic liquid crystal Metal Polymer chemistry Stereochemistry Organic chemistry Molecule Materials science Polymer Catalysis

Subject Areas

Liquid Crystal Research Advancements ·Electronic, Optical and Magnetic Materials ·Physical Sciences
Nonlinear Dynamics and Pattern Formation ·Computer Networks and Communications ·Physical Sciences
Synthesis and Properties of Aromatic Compounds ·Organic Chemistry ·Physical Sciences