Abstract
Abstract The crystal structure of the title compound, C17H13N5O4, has been determined by single crystal x-ray diffraction at room temperature. The molecule is not planar, with dihedral angles of 7.2(1)° between the quinoline ring and N-methylhydrazone group, and 17.45(2)° between the N-methylhydrazone group and the phenyl ring. The crystal parameters of this compound are as follows: monoclinic P 21/n, a=9.525(2)Å, b = 15.192(2) Å, c = 11.302(2) A, β = 94.722(3)°, V = 1629.8(6) Å3, Z = 4, Dx = 1.432 g/cm3, F(000) = 728, λ (MoKα) = 0.71070 Å, μ = 0.106 mm−1, Rint = 0.017. The structure was solved by SHELXS-86 and refined by SHELXL-93. R = 0.07 for 2438 observed reflections with I > 2σ (I).
Keywords
Monoclinic crystal system
Chemistry
Quinoline
Ring (chemistry)
Dihedral angle
Crystallography
Crystal structure
Molecule
Group (periodic table)
Crystal (programming language)
Planar
Stereochemistry
Hydrogen bond
Organic chemistry
Subject Areas
Synthesis and biological activity
·Organic Chemistry ·Physical Sciences
Synthesis and Characterization of Heterocyclic Compounds
·Organic Chemistry ·Physical Sciences
Metal complexes synthesis and properties
·Oncology ·Health Sciences
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