Journal Article

·2010

Synthesis and characterization of new D-π-D type Schiff base ligands and its complexes with Cobalt(II), Ruthenium(II)

İbrahim Erden YTU , Nebahat Demirhan YTU , Ulvi Avcata YTU

Russian Journal of Inorganic Chemistry

Abstract

A Schiff base ligands, N-{(1E,2E)-3-[4-(dimethylamino)phenyl]prop-2-en-1-ylidene}-1,10-phenanthrolin-5-amine(mpa) and (1E,2E)-3-[4-(dimethylamino)phenyl]acrylaldehyde9H-fluoren-9-ylidenehydrazone(mfh), have been synthesized from the reaction of 4,5-diazafluorenone-9-hydrazone and 5-amino-1,10-phenanthroline with 4-(dimethylamino)cinnamaldehyde. The Co(II) and Ru(II) complexes of the ligands were prepared and characterized. The metal-to-ligand ratio of the Co(II) complex was found to be 2: 1 and that of the Ru(II) complex was found to be 1: 1. The ligands and complexes have been characterized by FTIR, UV-visible, 1H NMR and fluorescence spectra, as well as, elemental analyses, TGA-DSC-DTG and mass spectra.

Keywords

Schiff base Chemistry Cinnamaldehyde Cobalt Ruthenium Hydrazone Ligand (biochemistry) Amine gas treating Proton NMR Medicinal chemistry Metal Polymer chemistry Mass spectrum Phenanthroline Stereochemistry Inorganic chemistry Mass spectrometry Catalysis Organic chemistry

Subject Areas

Metal complexes synthesis and properties ·Oncology ·Health Sciences
Lanthanide and Transition Metal Complexes ·Materials Chemistry ·Physical Sciences
Magnetism in coordination complexes ·Electronic, Optical and Magnetic Materials ·Physical Sciences

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