Journal Article

·2025 OPEN ACCESS

Synthesis, Structural and Mesomorphic Characterization of New Three-Ring Chalcone-Imine Derivatives with Polar End Groups

Ceren Can Karanlık YTU

Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi

Abstract

In this study, new chalcone-imine derivatives composed of three-benzene-ring central unit containing n-dodecyloxy group at one end and cyano or bromo group at other end have been synthesized. Chemical structures of the obtained derivatives have been clarified by spectral analyses (1H-, 13C/APT-NMR and FT-IR). The mesomorphic behaviour and optical textures of the derivatives have been observed by differential scanning calorimetry (DSC) and polarized optical microscopy (POM). It was determined that cyano-terminated chalcone-imine derivative (3a) exhibits enantiotropic SmA mesophase, characterized by thermal range of 19 ˚C and also a M mesophase, while bromo-terminated chalcone-imine derivative (3b) does not show any mesomorphic behaviour. This result emphasizes that the type and the nature of the polar end group has a huge impact on the liquid crystalline properties of the molecules.

Keywords

Differential scanning calorimetry Polar Group (periodic table) Derivative (finance) Characterization (materials science) Polarized light microscopy Crystallography Optical microscope

Subject Areas

Liquid Crystal Research Advancements ·Electronic, Optical and Magnetic Materials ·Physical Sciences
Synthesis and properties of polymers ·Polymers and Plastics ·Physical Sciences
Lipid Membrane Structure and Behavior ·Molecular Biology ·Life Sciences